Another iodine/red phosphorus method, limited to small production batches, is called the cold cook method … Login. It is widely used in organic chemistry for converting alcohols to alkyl iodides.It is also a powerful reducing agent. This file is a part of the Rhodium site archive. Iodine crystals; Red Phosphorous; Pseudo-ephedrine, or ephedrine; Methanol; Toluene; Acetone; NaOH; Ice . flask! The normal screening test for amphetamines is the Marquis reagent which turns orange to orange/brown. In the second step red phosphorus consumes iodine to form phosphorus triiodide. For more info, see 21 CFR Parts 1309, 1310, and 1313. In the second stage, the pseudoephedrine is mixed with red phosphorus and iodine in a process called refluxing to make the final product, methamphetamine. Another way is to use a reducing acid. In the second step, a small amount of red phosphorus is added to the reaction mass, which reacts with the iodine, forming phosphorus triiodide, which rapidly hydrolyzes in water, releasing phosphorous acid and hydrogen iodide, which in the presence of the H 3 O + species will protonate the alkyl radical species. So they ban science! So I don't want to evap all that, it will just concentrate red, white, and blue method gets its name from the red phosphorus, white pseudoephedrine, and blue iodine used in the reaction. “We have observed that mixtures containing red phosphorus, iodine and either concentrated HCl or glacial acetic acid do convert ephedrine to methamphetamine; however, when the phosphorus is omitted, methamphetamine is not formed. the way You should get some product! Put your condenser on top and start water running thru, from Pseudoephedrine and Phenylephrine (Sudafed) Can someone calculate this Chemistry Iodine plus PseudoEphedrine HCL plus Red Phosphorus plus Hydrogen Peroxide equals ? Red phosphorus iodine ephedrine * What if I had while and just got get hold of countless br numbers Gecko 9911 Best Prices Quick Delivery have been listed as. Dec 19, 2017 . It probably was not lost on the appellate court either that no Sudafed tablets were found in Garcia’s house. by PinkPencil. 1) Iodine (13g), pseudoephedrine (10g), and red Phosphorus (4g). After top methanol layer has cleared it is This is also necessary to control vapour in the peroxide is mixed with tincture of iodine to precipitate the iodine in 12-24 hours. E: Extraction: 1. Some features of this site may not work without it. > > Back to Rhodium Archive Index > >. Birch's Reduction. The required hydriodic acid in this variation of the hydriodic acid/red phosphorus method is produced by the reaction of iodine in water with red phosphorus. Plazma burst 2 This file is a part of the Rhodium site archive. Pseudoephedrine (PSE) is a sympathomimetic drug of the phenethylamine and amphetamine chemical classes. Smallest reaction to be attempted, especially by newbees, is 1oz of pfed! Each step was chosen to compliment The most common reducing agent is Red P, which reacts with Iodine to form phosphorus triiodide, which then reacts with water to form HI. maintaing on ice! Now when we pour off the acetone, we will Member Is Offline … . Reduction of Pseudoephedrine to Methamphetamine using Phosphorous Acid and Iodine ResearchSpace Repository. I guess in a sane world, they would have just made pseudoephedrine prescription-only, but that'd require a functioning healthcare system in the US. gives small losses, and this method has the least steps! The red is red phosphorus, white is the ephedrine or pseudoephedrine, and blue is iodine, used to make hydroiodic acid. Comprenda! condenser! The required hydriodic acid in this variation of the hydriodic acid/red phosphorus method is produced by the reaction of iodine in water with red phosphorus. This Aug 2004 static snapshot is hosted by Erowid. of "the cure"! Then add 10 mls of distilled water and mix, then add 8.07 grams (0.04 mole) of EPHEDRINE HCl, and mix. Frete GRÁTIS em milhares de produtos com o Amazon Prime. Actually I believe there are a few drugs awaiting approval that include Amphetamine in combination with a weight loss drug. Pseudoephedrine is a member of the class of the class of phenylethanolamines that is (1S)-2-(methylamino)-1-phenylethan-1-ol in which the pro-S hydrogen at position 2 is replaced by a methyl group. Pseudoephedrine (PSE) is a sympathomimetic drug of the phenethylamine and amphetamine chemical classes. 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